Chemical Shifts of NMR Solvents

britLine.GIF (1250 bytes)

This list was compiled from various sources.  No attempt has been made to verify its accuracy.

Name

MW

H shift (multiplicity)

C shift (multiplicity)

H shift of water

bp in deg C

acetic acid-d4

64.08

2.03 (5), 11.5 (1)

20.0 (7),  178.4(1)

 

118

acetone-d6

64.12

2.04(5)

206.0(1), 29.8(7)

 

57

acetonitrile-d3

44.07

1.93(5)

118.2(1), 1.3(7)

 

82

benzene-d6

84.15

7.15(1)

128.0(3)

.5

80

CDCl3

120.38

7.24(1)

77.0(3)

1.5

62

D2O

20.03

4.65(1)

 

 

101.4

DMF-d7

80.14

2.74(5), 2.91(5), 8.01(1)

162.7(3), 35.2(7), 30.1(7)

 

153

DMSO-d6

84.17

2.49(5)

39.5(7)

 

189

ethanol-d6

52.11

1.11(m), 3.55(1), 5.19(1)

56.8(5), 17.2(7)

 

79

methanol-d4

36.07

3.30(5), 4,78(1)

49.0(7)

 

65

CD2Cl2

89.94

5.32(3)

53.8(5)

 

40

pyridine-d5

84.13

7.19(1), 7.55(1), 8.71(1)

149.9(3), 135.5(3), 123.5(5)

 

116

THF-d8

80.16

1.73(1), 3.58(1)

67.4(5), 25.3(1)

 

66

toluene-d8

100.19

2.09(5), 6.98(m), 7.00(1), 7.09(m)

137.5(1), 128.9(3), 128.0(3), 125.2(3), 20.4(7)

 

111

TFA-d1

115.03

11.5(1)

164.2(4), 116.6(4)

 

72

 

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